Laboratory test:
1. Chemical Composition test
- Lime saturation Factor (LSF): This is the ratio of Lime% to % of Silica, Alumina and Iron oxide. This value should be in between 1.02-0.66.
Cao - 0.7SO3
( 2.8SiO2+1.2Al2O3+0.65Fe2O3)
- Ratio of % Alumina (Al2O3) to Iron oxide (Fe2O3) shall not be less than 0.66
- Wt. of Insoluble residue shall not be more than 4%
- Wt. of Magnesia (MgO) shall not be more than 6%
- Shall not more than 5% loss on ignition.
2. Normal Consistency Test
- 500 gm of cement @27 0C 90% Humidity mix with water( 23-24% wt of cement).
- Fill paste in the mould having dimension 80 mm dia , 40 mm depth
- Normal Consistency if define as the cement paste which allow penetration of Vicat Plunger(10 mm dia & 500 mm Length) 5 to 7 mm from bottom or 33 mm to 35 mm from top.
- Change the % of water till above given criteria achieve. that % of water is called Normal Consistency of Cement.
- Vicat Plunger : 300 gm , 50 mm length, 10 mm dia
3. Intial Setting Time
- Initial setting time is the time after which cement start losing its plasticity.
- It should not be less than 30 min and more than 60 min for OPC
- Take 500 gm of cement @27 0C 90% Humidity mix with water ( 0.85 Normal consistency of cement).
- Time at which Vicat Plunger having 1 mm square size penetrate 5 mm to 7 mm from bottom.
4. Final Setting Time
- Final setting time is the time cement paste lost complete plasticity and start hardening.
- Its should not be more than 10 Hr for OPC (ordinary Portland cement).
- Needle makes impression but collar fail to do.
- Procedure is same as above , dimension of Vicat is Annular Collar of 10 mm size.
5. Soundness Test
- Soundness is determine by "Le Chatellier's Test if Lime(CaO) is in excess amount and Autoclave Test if Lime and Magnesia(MgO) both are in excess amount.
- Le- Chatellier's is the split cylinder method value should not be more than 10 mm. Split Cylinder Depth and Height of Cylinder having arm is 30 mm both.
- Autoclave Test value should not be exceed 0.8% of length dimension or 25 mm. pressure applied 21kg/cm2 for period of 3 Hr.
thanks
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